IGSNRR OpenIR
Study on the kinetic model, thermodynamic and physicochemical properties of Glycyrrhiza polysaccharide by ultrasonic assisted extraction
Wang, Yonggang1; Zhang, Xuan1; Ma, Xueqing2; Zhang, Kang3; Li, Shaowei4; Wang, Xinjian1; Liu, Xiaofeng1; Liu, Jichao1; Fan, Wenguang1; Li, Yuanli1; Li, Qingyang5; Zhu, Xinqiang2
2019-03-01
Source PublicationULTRASONICS SONOCHEMISTRY
ISSN1350-4177
Volume51Pages:249-257
Corresponding AuthorWang, Yonggang(412316788@163.com) ; Li, Shaowei(leesw@igsnrr.ac.cn)
AbstractThe extraction process of crude polysaccharides from Glycyrrhiza (GP) by ultrasonic assisted hot water method was established according to the optimized kinetic model based on Fick's second law of diffusion, and thermodynamic action was analyzed. Physicochemical properties of GP including the apparent viscosity, thermo-stability and antioxidant activities etc. were determined by ultraviolet spectrophotometry and differential scanning calorimetry (DSC). Characteristic function groups and surface structure also were analyzed by Fourier infrared spectroscopy (FT-IR), scanning electron microscopy (SEM) and atomic force microscopy (AFM), respectively. The results showed the extraction kinetic curves of GP showed good linear correlation with the linear correlation coefficients (R-2) of equal or greater than 0.90 based on Fick's second law of diffusion, and the maximum yield of 3.53% was obtained at 343.15 K and ultrasonic power 600 W with material-liquid ratio of 1:15 for 60 min. Gibbs free energy change (Delta G(m) > 0) indicated that the extraction process was endergonic and not spontaneous. GP was confirmed a kind of acidic pyran polysaccharide with small bubble-like holes internally. The GP viscosity increased with the increase of concentration and then gradually decreased with the enhancement of shear rate. GP showed good thermal stability along with two stages of mass loss by DSC analysis. The antioxidant activity experiments suggested that the higher the concentration of GP, the stronger its reduction power.
KeywordGlycyrrhiza uralensis Fisch Ultrasonic-assisted extraction Kinetic model Thermodynamics analysis Physicochemical properties
DOI10.1016/j.ultsonch.2018.10.012
WOS KeywordVITRO ANTIOXIDANT ACTIVITY ; STRUCTURAL-CHARACTERIZATION ; ANTITUMOR-ACTIVITY ; OPTIMIZATION ; PURIFICATION ; EXOPOLYSACCHARIDES ; DEGRADATION ; LICORICE
Indexed BySCI
Language英语
Funding ProjectNational Natural Science Foundation of China[31460032] ; National Natural Science Foundation of China[81660581] ; National Natural Science Foundation of China[31760028] ; Youth talent support program of Lanzhou University and Technology[2018]
Funding OrganizationNational Natural Science Foundation of China ; Youth talent support program of Lanzhou University and Technology
WOS Research AreaAcoustics ; Chemistry
WOS SubjectAcoustics ; Chemistry, Multidisciplinary
WOS IDWOS:000454375900029
PublisherELSEVIER SCIENCE BV
Citation statistics
Document Type期刊论文
Identifierhttp://ir.igsnrr.ac.cn/handle/311030/51264
Collection中国科学院地理科学与资源研究所
Corresponding AuthorWang, Yonggang; Li, Shaowei
Affiliation1.Lanzhou Univ Technol, Sch Life Sci & Engn, Lanzhou 730050, Gansu, Peoples R China
2.Chinese Acad Agr Sci, State Key Lab Vet Etiol Biol, Natl Foot & Mouth Dis Reference Lab, Lanzhou Vet Res Inst, 1 Xujiaping, Lanzhou 730046, Gansu, Peoples R China
3.Chinese Acad Agr Sci, Lanzhou Inst Husb & Pharmaceut Sci, Lanzhou 730050, Gansu, Peoples R China
4.Chinese Acad Sci, Inst Geog Sci & Nat Resources Res, Beijing 100101, Peoples R China
5.Cent S Univ, Xiangya Sch Med, Changsha 410000, Hunan, Peoples R China
Recommended Citation
GB/T 7714
Wang, Yonggang,Zhang, Xuan,Ma, Xueqing,et al. Study on the kinetic model, thermodynamic and physicochemical properties of Glycyrrhiza polysaccharide by ultrasonic assisted extraction[J]. ULTRASONICS SONOCHEMISTRY,2019,51:249-257.
APA Wang, Yonggang.,Zhang, Xuan.,Ma, Xueqing.,Zhang, Kang.,Li, Shaowei.,...&Zhu, Xinqiang.(2019).Study on the kinetic model, thermodynamic and physicochemical properties of Glycyrrhiza polysaccharide by ultrasonic assisted extraction.ULTRASONICS SONOCHEMISTRY,51,249-257.
MLA Wang, Yonggang,et al."Study on the kinetic model, thermodynamic and physicochemical properties of Glycyrrhiza polysaccharide by ultrasonic assisted extraction".ULTRASONICS SONOCHEMISTRY 51(2019):249-257.
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